Sandwich Technique for Small Sample Volumes

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Contents

Overview

Allows sandwiching of sample between user-selected volumes of wash solvent. In addition, after a user-specified delay, the injection valve is toggled back to the Load position and washed using the same solvent. This will be done after the standard syringe and valve wash sequence.

The pump system can get an injected signal that allows its program to increase flow rate for specific period of time to permit rapid introduction of sandwiched sample onto the column.

Benefits

To control small sample volumes for capillary injections. Can help minimize sample carryover since the last solvent that the valve sees is wash solvent


Project Ref: H1066

For other cost/time saving measures consider:

  • LEAP offers multiple choices of Valve Self Wash Stations to aid in cleaning the valve [1]
  • Dual Channel Serial Injection with Front Cut (M-002) using Analyst and ICC-CE [2]
  • Dual Channel Parallel Injection (M-003) using Cycle Composer Software and Analyst [3]
  • “Look Ahead”, sample prep before injection (M-004) using LEAP Shell Software [4]
  • Dual Channel Parallel Injection (M-005) using LEAP Shell software [5]
  • Summary of LC Multi Valve Applications [6]
  • LEAP Shell Software and application for custom injections and scheduling [7]

Contact LEAP

For additional information about this technique please contact LEAP Technologies for detailed information



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