GC Headspace
From LEAP
| GC Headspace |
| Application Type | |
| STANDARD | |
| Application ID | |
| GC90210 | |
| Description | |
| GC headspace sample processing with ChemStation. |
Contents |
Abstract
A simple and fairly standardized technique of extracting volatile and semi-volatile substances from raw samples in liquid or solid form is headspace analyzes [1]. A sample is placed in a vial that is sealed by a septum and cap and heated in an incubator for a specific time. Once the content of the vial has reached equilibrium a sampled is extracted and injected into the injection port of a GC. LEAP’s specific equipment the CTC CombiPAL[2] performs all the tasks for this extraction method unattended. For a sequence of samples up to 96 the Combi PAL[3] will schedule the vials to be in the incubator/agitator for the same amount of time before a precise sample of headspace gas is extracted by a heated syringe system for a subsequent appropriate injection into a GC. Many variables are programmable over a validated range. 1ml, 2.5ml and 5ml syringes and a solvent-less solid phase micro extraction system are the tools that can be mounted in the injection head.
CombiPAL Headspace mode with Heated Syringe
- 30°C-150°C
- Available in 1ml/ 2.5ml/ 5ml
Screenshots
 LEAP Shell Method |
 Sample queue |
 PAL sample prep method |
 PAL sample injection method |
Photos
 Sample vial tray |
 Magnetic tool tip |
 Bar code reader |
 Agitator |
 Agitator |
 Vial in transfer |
Agilent 6890 GC / 5975C VL MSD |
Some Advantages of Headspace Analysis
- Limited sample preparation
- Improves detection limits
- Reduction in method development times
- Reduction of matrix interference from sample matrix
- Extended life of the GC column
- Reduction of instrument down time
Accessories
Agitation of Samples Agitation_of_Samples
Multiple Headspace Extractions Option Multi_Headspace_Extractions
ITEX-2 Option ITEX-2
Venting with an inert gas before Headspace Vent Tool
Barcode Reading with LEAP Shell software Bar Code Reading
CombiPAL [4]
Useful links
General Information on Gas Chromatography
Videos
Movie of the COMBI PAL with Headspace in action. [5]
LEAP provides automated workstation instrumentation solutions based on the LEAP CTC PAL X, Y, Z syringe only autosampler robot from LEAP Technologies. This extremely flexible, precise, and adaptable liquid handling robotic platform is available in a variety of lengths and options depending on the requirements of your sample preparation and injections for your UHPLC, LC or GC chromatography.LEAP offers full support and service for the PAL platform in addition to being able to write custom macros, cycles, and scheduling to your applications. We're proud that LEAP is known as a productivity improver for laboratories, and we have big plans to even make government labs in agencies such as FDA, USDA, EPA, FBI, Armed Forces, Homeland Security and others function more efficiently. Robotic sample prep equipment works well in government labs and challenges lab technicians to keep feeding those more samples. Analytical equipment such as chromatographs and mass spectrometers are expensive devices and also expensive to maintain. The least an owner can do is to keep them running and analyze samples around the clock. LEAP has most of its lab automation robots under GSA contract and is eager to service and maintain everything it sells to keep your expensive lab equipment running around the clock. Please contact LEAP Technologies on how we can help you get maximized throughput with flexible pipetting automation solutions.
Contact LEAP
 Contact LEAP
For additional information about LEAP and the PAL Platform, please contact LEAP Technologies. |
