Monitoring of Polymerization reactions
From LEAP
(Difference between revisions)
| Line 9: | Line 9: | ||
=== Overview === | === Overview === | ||
| - | + | This application uses a re-circulating pump to continuously flow fluid from a reactor vessel to the HPLC valve of the PAL. At specified timed intervals the HPLC valve toggles so that the loop contain the the reaction fluid is taken tmeporarily out of flow, and the contents of the loop is sampled using a syringe and placed in a storage vial for later analysis. | |
| - | The whole system can be placed upon a moveable cart and positioned | + | The whole system can be placed upon a moveable cart and positioned close to any reactor. |
| + | |||
| + | Flow Diagram in default position: | ||
[[Image:Promerus_Flow_Diagram.png]] | [[Image:Promerus_Flow_Diagram.png]] | ||
| + | |||
| + | Flow diagram when sampling: | ||
| + | |||
| + | [[Image:Promerus_Flow_Diagram_2.png]] | ||
Revision as of 15:54, 19 February 2009
| Monitoring of Polymerization reactions |
| Application Type | |
| SPECIAL | |
| Application ID | |
| Description | |
| Timed sampling of polymer reactor vessel under high pressure and temperature. |
Overview
This application uses a re-circulating pump to continuously flow fluid from a reactor vessel to the HPLC valve of the PAL. At specified timed intervals the HPLC valve toggles so that the loop contain the the reaction fluid is taken tmeporarily out of flow, and the contents of the loop is sampled using a syringe and placed in a storage vial for later analysis.
The whole system can be placed upon a moveable cart and positioned close to any reactor.
Flow Diagram in default position:
Flow diagram when sampling:
Screen Shots
 Customized Sample List |
 Runtime reporting of status in Queue |
Further Documentation
LEAP Application Note: Reaction_Monitoring_App_Note.pdf
